Download Catalysts for Fine Chemical Synthesis. Regio- and Stereo- by Stanley M. Roberts, John Whittall PDF

By Stanley M. Roberts, John Whittall

Quantity five within the Catalysts for high-quality Chemical Synthesis sequence describes new tactics for the regio- and stereo-controlled changes of compounds concerning oxidation or aid reactions. It describes a variety of catalysts, together with organometallic structures, biocatalysts and biomimetics. This quantity additionally contains descriptions of a number of conversions, together with: Baeyer-Villiger oxidations; Epoxidation reactions; Hydroxylation reactions; Oxidation of alcohols to aldehydes, ketones and carboxylic acids; relief of ketones; and aid of alkenes together with α, β-unsaturated carbonyl compounds. The ebook could be a big textual content for working towards man made natural chemists in and academia.

  • Protocols are written in a typical layout through the authors who've came across them
  • Hints, assistance and safeguard suggestion (where applicable) is given to make sure that the methods are reproducible
  • Indications are given as to the diversity of beginning fabrics used and, the place acceptable, comparisons to replacement methodology
  • Includes suitable references to the first literature.

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Extra resources for Catalysts for Fine Chemical Synthesis. Regio- and Stereo- Controlled Oxidation and Reductions

Sample text

5. R. J. An Enantioselective Synthesis of b2-Amino Acid Derivatives. Tetrahedron Asymmetry 2005, 16, 1309–1319. 6. , Marinetti, A. and Larcheveˆque, M. An Efficient Synthesis of Chiral Cyclic b-Amino Acid via Asymmetric Hydrogenation. Synlett. 2004, 15, 2766–2770. 7. Kubryk, M. B. Application of the Asymmetric Hydrogenation of Enamines to the Preparation of a b-Amino Acid Pharmacophore. Tetrahedron Asymmetry 2006, 17, 205–209. 8. Hoge, G. Presentation at Modern Synthetic Methods Conference, Princetown, 2005.

An Enantioselective Synthesis of b2-Amino Acid Derivatives. Tetrahedron Asymmetry 2005, 16, 1309–1319. 6. , Marinetti, A. and Larcheveˆque, M. An Efficient Synthesis of Chiral Cyclic b-Amino Acid via Asymmetric Hydrogenation. Synlett. 2004, 15, 2766–2770. 7. Kubryk, M. B. Application of the Asymmetric Hydrogenation of Enamines to the Preparation of a b-Amino Acid Pharmacophore. Tetrahedron Asymmetry 2006, 17, 205–209. 8. Hoge, G. Presentation at Modern Synthetic Methods Conference, Princetown, 2005.

57 ..... 59 ..... 60 ..... 61 ..... 62 ..... 63 ..... 64 65 (QUINOXP*) AS A LIGAND FOR RHODIUM-CATALYZED ASYMMETRIC ............ Synthesis of (R)-tert-Butyl(hydroxymethyl)methylphosphine–borane. Synthesis of (R)-Benzoyloxy(tert-butyl)methylphosphine–borane . . Synthesis of (S)-tert-Butylmethylphosphine–borane. . . . . . . (R,R)-2,3-Bis(tert-butylmethylphosphino)quinoxaline (QuinoxP*) . . Asymmetric hydrogenation of Methyl (E)3-acetylamino-2-butenoate catalyzed by Rh(I)-(R,R)-2,3-Bis(tert-butylmethylphosphino)quinoxaline .

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